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Development of Novel Bicyclopentanes (BCP) Bioisosteres From Bench Stable [1.1.1]-Propellane Precursors PhD Bicyclo-[1.1.1]-pentanes (BCPs) are an exciting class of strained, sp3 rich carbon. While their initial use was in the materials sector, recent impact... Read more has been in medicinal chemistry, drug development and the agrochemical sector. Their appeal is due to a unique 3-D structure, a direct consequence of its high sp3 carbon content, and has led to its use as a bioisosteres for the tert-butyl group, internal alkynes and significantly, mono- and disubstituted arenes. Their synthesis is accomplished using hetero- or homolytic cleavage and relies on the inherent strain in the central carbon-carbon bond of [1.1.1]-propellane. However, the practical isolation and storage of [1.1.1]-propellane is very problematic; it is isolated as a solution in ethereal solvents, it must be cryogenically stored, and should be used before its rapid degradation. In this project we will pioneer a stable crystalline alternatives of [1.1.1]-propellane. Functionalization will be explored using several nucleophiles, providing orthogonal 1,3-disubstituted-[1.1.1]-bicyclopentane (BCP) precursors amenable to subsequent cross-coupling reactions (e.g., transition metal and photoredox mediated). This methodology will provide a superior synthetic approach to 1,3-disubstituted BCPs, with far less waste, as well as delivering stable crystalline BCP precursors. This project will significantly increase the synthetic scope of BCPs compared to current strategies, as well as providing an excellent training platform to the prospective PhD candidate in our new state-of-the-art laboratories here at Loughborough. Read less
Program overview
Main Subject
Chemistry
Degree
PhD
Study Level
PHD
Study Mode
On Campus
Development of Novel Bicyclopentanes (BCP) Bioisosteres From Bench Stable [1.1.1]-Propellane Precursors PhD Bicyclo-[1.1.1]-pentanes (BCPs) are an exciting class of strained, sp3 rich carbon. While their initial use was in the materials sector, recent impact... Read more has been in medicinal chemistry, drug development and the agrochemical sector. Their appeal is due to a unique 3-D structure, a direct consequence of its high sp3 carbon content, and has led to its use as a bioisosteres for the tert-butyl group, internal alkynes and significantly, mono- and disubstituted arenes. Their synthesis is accomplished using hetero- or homolytic cleavage and relies on the inherent strain in the central carbon-carbon bond of [1.1.1]-propellane. However, the practical isolation and storage of [1.1.1]-propellane is very problematic; it is isolated as a solution in ethereal solvents, it must be cryogenically stored, and should be used before its rapid degradation. In this project we will pioneer a stable crystalline alternatives of [1.1.1]-propellane. Functionalization will be explored using several nucleophiles, providing orthogonal 1,3-disubstituted-[1.1.1]-bicyclopentane (BCP) precursors amenable to subsequent cross-coupling reactions (e.g., transition metal and photoredox mediated). This methodology will provide a superior synthetic approach to 1,3-disubstituted BCPs, with far less waste, as well as delivering stable crystalline BCP precursors. This project will significantly increase the synthetic scope of BCPs compared to current strategies, as well as providing an excellent training platform to the prospective PhD candidate in our new state-of-the-art laboratories here at Loughborough. Read less
Admission Requirements
3.2+
6.5+
92+
Applicants should have or expect to achieve at least a 2:1 honours degree (or equivalent international qualification) in chemistry.
3 Years
Jan
Apr
Scholarships
Selecting the right scholarship can be a daunting process. With countless options available, students often find themselves overwhelmed and confused. The decision can be especially stressful for those facing financial constraints or pursuing specific academic or career goals.
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Development of Novel Bicyclopentanes (BCP) Bioisosteres From Bench Stable [1.1.1]-Propellane Precursors PhD![Development of Novel Bicyclopentanes (BCP) Bioisosteres From Bench Stable [1.1.1]-Propellane Precursors PhD](/themes/custom/tu_d8/images/uniprofile/link_white.svg)
Loughborough University, Loughborough, United Kingdom
# 301-350QS Subject Rankings
36 monthsProgram duration
ChemistryMain Subject Area
Program overview
Main Subject
Chemistry
Degree
PhD
Study Level
PHD
Study Mode
On Campus
Bicyclo-[1.1.1]-pentanes (BCPs) are an exciting class of strained, sp3 rich carbon. While their initial use was in the materials sector, recent impact...
Read more has been in medicinal chemistry, drug development and the agrochemical sector. Their appeal is due to a unique 3-D structure, a direct consequence of its high sp3 carbon content, and has led to its use as a bioisosteres for the tert-butyl group, internal alkynes and significantly, mono- and disubstituted arenes.
Their synthesis is accomplished using hetero- or homolytic cleavage and relies on the inherent strain in the central carbon-carbon bond of [1.1.1]-propellane. However, the practical isolation and storage of [1.1.1]-propellane is very problematic; it is isolated as a solution in ethereal solvents, it must be cryogenically stored, and should be used before its rapid degradation.
In this project we will pioneer a stable crystalline alternatives of [1.1.1]-propellane. Functionalization will be explored using several nucleophiles, providing orthogonal 1,3-disubstituted-[1.1.1]-bicyclopentane (BCP) precursors amenable to subsequent cross-coupling reactions (e.g., transition metal and photoredox mediated). This methodology will provide a superior synthetic approach to 1,3-disubstituted BCPs, with far less waste, as well as delivering stable crystalline BCP precursors.
This project will significantly increase the synthetic scope of BCPs compared to current strategies, as well as providing an excellent training platform to the prospective PhD candidate in our new state-of-the-art laboratories here at Loughborough. Read less
Program overview
Main Subject
Chemistry
Degree
PhD
Study Level
PHD
Study Mode
On Campus
Bicyclo-[1.1.1]-pentanes (BCPs) are an exciting class of strained, sp3 rich carbon. While their initial use was in the materials sector, recent impact...
Read more has been in medicinal chemistry, drug development and the agrochemical sector. Their appeal is due to a unique 3-D structure, a direct consequence of its high sp3 carbon content, and has led to its use as a bioisosteres for the tert-butyl group, internal alkynes and significantly, mono- and disubstituted arenes.
Their synthesis is accomplished using hetero- or homolytic cleavage and relies on the inherent strain in the central carbon-carbon bond of [1.1.1]-propellane. However, the practical isolation and storage of [1.1.1]-propellane is very problematic; it is isolated as a solution in ethereal solvents, it must be cryogenically stored, and should be used before its rapid degradation.
In this project we will pioneer a stable crystalline alternatives of [1.1.1]-propellane. Functionalization will be explored using several nucleophiles, providing orthogonal 1,3-disubstituted-[1.1.1]-bicyclopentane (BCP) precursors amenable to subsequent cross-coupling reactions (e.g., transition metal and photoredox mediated). This methodology will provide a superior synthetic approach to 1,3-disubstituted BCPs, with far less waste, as well as delivering stable crystalline BCP precursors.
This project will significantly increase the synthetic scope of BCPs compared to current strategies, as well as providing an excellent training platform to the prospective PhD candidate in our new state-of-the-art laboratories here at Loughborough. Read less
Admission Requirements
Scholarships
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QS subject rankings
Subject: Chemistry
Ranking criteria
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Cell Mechanics and Tumour Growth PhD
Cellular Automaton to Model Rapid Crystal Growth and Recrystallisation PhD
Cognitive Monitoring of Human Operators using Multi-modal Artificial Intelligence PhD
Continuous Manufacturing Of Nano-Assemblies For Mrna Based Therapies And Vaccines: From Batch To Industry Scale PhD
Countering Cyberattacks in Autonomous Vehicles PhD
Cryptographic Primitives for Symmetric Cryptography PhD
Crystallisation with 3D Printing Template and Hydrogel Templates PhD
Data and AI Powered Turbulence Modelling for Fusion Energy Cooling Flows PhD
Design and fabrication Custom Foot Orthotics PhD
Design of Programmable Mechanical Metamaterials PhD
Developing Diffusion Models for Electric Vehicle: Spatial-temporal analysis and Policy Evaluation PhD
Developing Natural Surfactants from Biomass for Industrial Applications PhD
Development of New Digital Technologies and Generative Artificial Intelligence Tools For The Next Generation Green-By-Design and Sustainable Pharmaceuticals PhD
Development of Robust Wall Modelling for Practical Aerodynamic High Fidelity Prediction Phd
Dynamic Deformation, Damage and Fracture Of Composites PhD
Energy Efficiency Optimisation of Electric Vehicles In Dynamic Driving Scenarios PhD
Engineering New Materials for Solid-State Cooling Phd
Enhancing Human-Robot Interaction: Leveraging Artificial Intelligence for Emotional Intelligence in Robotics PhD
Unveiling Molecular Mechanisms of the Beneficial Impact of Exercise on Cancer Metabolism PhD
Using the Metabolome to Study Aging and Geroprotectors in 3D Cell Models PhD
Visual Data Mining on Proteins and Biomedicine Crystallisation PhD
Waste-derived Bioplastics for a Circular and Sustainable Food Packaging Economy PhD
Life Sciences and Medicine (5)
Adaptive and Predictive Computational Modelling of Biomaterials: A Digital Twin Framework for Next-Generation Personalised Healthcare PhD
Adaptive and Predictive Computational Modelling of Biomaterials: A Digital Twin Framework for Next-Generation Personalised Healthcare PhD
Biomarkers of Aging PhD
Biomarkers of Aging PhD
Developing Prescription Guidelines for Passive Heat Therapy PhD
Developing Prescription Guidelines for Passive Heat Therapy PhD
Does Socialised Real-Life Body Exposure Promote Body Image Positivity PhD
Does Socialised Real-Life Body Exposure Promote Body Image Positivity PhD
Energy Dissipation In Human Soft Tissue During Impacts PhD
Energy Dissipation In Human Soft Tissue During Impacts PhD
Natural Sciences (13)
Accelerated Screening and Synthesis of New Chemotherapeutic Agents for Pancreatic Cancer PhD
Accelerated Screening and Synthesis of New Chemotherapeutic Agents for Pancreatic Cancer PhD
Bespoke Organometallic Compounds for Anticancer Studies PhD
Bespoke Organometallic Compounds for Anticancer Studies PhD
Bio-based Sustainable Materials for Autonomous Thermal Management in Wearables PhD
Bio-based Sustainable Materials for Autonomous Thermal Management in Wearables PhD
Biomimmetic Catalytic Asymmetric Synthesis of the Bisorbicillinoids and Related Products PhD
Biomimmetic Catalytic Asymmetric Synthesis of the Bisorbicillinoids and Related Products PhD
Climate and Ecological Transitions Hub Studentship PhD
Climate and Ecological Transitions Hub Studentship PhD
Coherent State Methods in Spectral Asymptotics PhD
Coherent State Methods in Spectral Asymptotics PhD
Computational Modelling of Sustainable Alloys PhD
Designing Classroom Tasks To Improve Students’ Learning Of Mathematics PhD
Developing Novel Antibiofilm Coatings for Sustainable Biofilm-Free Surfaces PhD
Development of Hybrid Microcomb Sources with Topologically Protected Dark Resonances for Simultaneous Classical and Quantum PhD
Development of Novel Bicyclopentanes (BCP) Bioisosteres From Bench Stable [1.1.1]-Propellane Precursors PhD
Digital Twins for Biofilm Management PhD
Dispersionless Integrable Systems In 2+1 Dimensions PhD
Social Sciences and Management (5)
An Evaluation of Erasmus+ Sport Projects and Their Impact on EU Sport Policy Development PhD
An Evaluation of Erasmus+ Sport Projects and Their Impact on EU Sport Policy Development PhD
Climate Change, Work Design and Worker Wellbeing Phd
Climate Change, Work Design and Worker Wellbeing Phd
Communication and Social Change (CSC) Hub Studentship PhD
Communication and Social Change (CSC) Hub Studentship PhD
Enhancing Motivation in Sport and Exercise Contexts PhD
Enhancing Motivation in Sport and Exercise Contexts PhD
Out of School Youth Provision: An Analysis of Funding and Operational Resilience within the Sector PhD
Out of School Youth Provision: An Analysis of Funding and Operational Resilience within the Sector PhD